Title:
Quantitative imaging of subsurface structures and mechanical properties at nanoscale using atomic force microscope

dc.contributor.advisor Degertekin, F. Levent
dc.contributor.author Parlak, Zehra en_US
dc.contributor.committeeMember Elisa Riedo
dc.contributor.committeeMember Hongwei Wu
dc.contributor.committeeMember Jennifer Michaels
dc.contributor.committeeMember Oliver Brand
dc.contributor.department Electrical and Computer Engineering en_US
dc.date.accessioned 2011-03-04T20:20:39Z
dc.date.available 2011-03-04T20:20:39Z
dc.date.issued 2010-11-15 en_US
dc.description.abstract This dissertation focuses on quantitative subsurface and mechanical properties imaging potential of AFM probes. Extensive modeling of AFM probes are presented for thorough understanding of capabilities and limitations of current techniques, these models are verified by various experiments, and different methods are developed by utilizing force-sensing integrated read-out active tip (FIRAT), which is an active AFM probe with broad bandwidth. For quantitative subsurface imaging, a 3-D FEA model of AFM tip-sample contact is developed and this model can simulate AFM tip scan on nanoscale-sized buried structures. FIRAT probe, which is active and broadband, is utilized for interaction forces imaging during intermittent contact mode and mechanical characterization capability of this probe is investigated. It is shown that probe dynamics, stiffness, stiffness ambiguity, assumed contact mechanics, and noise are important parameters for the accuracy of mechanical properties imaging. An active tip control mechanism is introduced to limit contact forces during intermittent contact mode. In addition to these, a combined ultrasonic AFM and interaction forces imaging method is developed and modeled to solve the reduced elasticity measurement sensitivity on composite materials. This method is capable of imaging a broader range of elasticity on combination samples such as metal nanoparticles in polymers at nanoscale. en_US
dc.description.degree Ph.D. en_US
dc.identifier.uri http://hdl.handle.net/1853/37181
dc.publisher Georgia Institute of Technology en_US
dc.subject Atomic force microscope en_US
dc.subject AFM en_US
dc.subject Ultrasonic AFM en_US
dc.subject Nanoscale subsurface imaging en_US
dc.subject Mechanical property imaging en_US
dc.subject Tapping mode en_US
dc.subject FIRAT en_US
dc.subject.lcsh Scanning probe microscopy
dc.subject.lcsh Imaging systems
dc.title Quantitative imaging of subsurface structures and mechanical properties at nanoscale using atomic force microscope en_US
dc.type Text
dc.type.genre Dissertation
dspace.entity.type Publication
local.contributor.advisor Degertekin, F. Levent
local.contributor.corporatename School of Electrical and Computer Engineering
local.contributor.corporatename College of Engineering
relation.isAdvisorOfPublication 9afd92fe-bb98-4c83-b8ac-fc596320991a
relation.isOrgUnitOfPublication 5b7adef2-447c-4270-b9fc-846bd76f80f2
relation.isOrgUnitOfPublication 7c022d60-21d5-497c-b552-95e489a06569
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