Title:
Liquid-phase synthesis of thiol-derivatized silver nanocrystals
Liquid-phase synthesis of thiol-derivatized silver nanocrystals
| dc.contributor.author | Murthy, Srihari | |
| dc.contributor.author | Bigioni, Terry P. | |
| dc.contributor.author | Wang, Z. L. (Zhong Lin) | |
| dc.contributor.author | Khoury, Joseph T. | |
| dc.contributor.author | Whetten, R. L. | |
| dc.date.accessioned | 2006-04-17T15:01:21Z | |
| dc.date.available | 2006-04-17T15:01:21Z | |
| dc.date.issued | 1997 | |
| dc.description.abstract | A liquid-phase method is reported for the preparation of dodecanethiol-derivatized silver nanocrystals. Toluene sols of this material maintain as sols in air at room temperature at least on the timescale of months. X-ray diffraction (XRD) and transmission electron microscopy (TEM) are used to obtain size and structural information about the nanocrystal core while solubility properties and energy dispersive X-ray spectroscopy (EDS) are used to identify the passivating layer. Laser desorption time-of-flight mass spectra (LDTOFMS) of this material show broad peaks in the mass range from 40 to 300 kamu. These results are consistent with the synthesized material being a dodecanethiol-derivatized silver nanocrystal material with a mean crystalline silver core of 3.1 ± 0.6 nm. | en |
| dc.format.extent | 480861 bytes | |
| dc.format.mimetype | application/pdf | |
| dc.identifier.citation | "Liquid-Phase Synthesis of Thiol-Derivatized Silver Nanocrystals", S. Murthy, T.P. Bigioni, Z.L. Wang, J.T. Khoury and R.L. Whetten, Mater. Lett., 30 (1997) 321-325. | en |
| dc.identifier.uri | http://hdl.handle.net/1853/9316 | |
| dc.language.iso | en_US | en |
| dc.publisher | Georgia Institute of Technology | en |
| dc.subject | Silver nanocrystals | en |
| dc.subject | Thiol-derivatization | en |
| dc.subject | Self-assembled monolayers | en |
| dc.subject | Nanoscale metal-organic composites | en |
| dc.subject | Transmission electron microscopy | en |
| dc.title | Liquid-phase synthesis of thiol-derivatized silver nanocrystals | en |
| dc.type | Text | |
| dc.type.genre | Article | |
| dspace.entity.type | Publication | |
| local.contributor.corporatename | School of Materials Science and Engineering | |
| local.contributor.corporatename | College of Engineering | |
| relation.isOrgUnitOfPublication | 21b5a45b-0b8a-4b69-a36b-6556f8426a35 | |
| relation.isOrgUnitOfPublication | 7c022d60-21d5-497c-b552-95e489a06569 |